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 Evaluación de diferentes reactivos aplic= ados en la precipitación del oro

 

Evaluation of different reagents applied in gold precipitation

 

Javier Ignacio Briones García.[1], Norma del Rocío Toledo Castillo.[2], & Teresita Jackelin Mejía Reinoso.[3]

 

Recibido: 11-02-2020 / Revisado: 18-03-2020 /Aceptado: 04-04-2020/ Publicado: 08-05-2= 020

 

Abstract.                               DOI: https://doi.org/10.33262/concienciadigita= l.v3i2.1.1234

 

In the present research work, 4 different reagents used in the precipitation of gold from solutions are evaluated, two of them used in a classical way such as sodium bisulfite and ferrous sulfate, against two rare species such as sugar and starch. In the experimental part, alluvial gold was mixed with sandy river material to ass= ess the efficiency of the reagents, the leaching of the gold was carried out wi= th aqua regia, this being a particularly strong oxidizing agent formed by the mixture of nitric acid and hydrochloric acid In a 3: 1 volume ratio respectively, statistical programming software was applied in the data analysis, with sugar being the highest precipitating agent.

 

Keywords: Precipitation. Gold. Sodium bisulfite. Ferrous sulfate. Sugar. Starch

 

Resumen.

En el presente trabajo de investigación se evalúa 4 diferentes reactivos utilizados en la precipitación del oro desde soluciones, dos de ellos utilizados de forma clásica como son el bisulfito de sodio y el sulfato ferroso, frente a dos especies poco comunes como el azúcar y el almidón. En= la parte experimental se mezcló oro de aluvión con material arenoso de río para valorar la eficiencia de los re= activos, la lixiviación del oro se llevó a cabo con agua regia siendo este un agente oxidante particularmente fuerte formado por la mezcla de ácido nítrico y ác= ido clorhídrico en una proporción de volumen 3:1 respectivamente, en el análisi= s de datos se aplicó un software de programación estadístico, siendo el azúcar e= l mayor agente precipitante.

 

Palabras claves: Precipitaci= ón. Oro. Bisulfito de sodio. Sulfato ferroso. Azúcar. Almidón.

Intro= ducción.

El oro ha sido durante mucho tiempo tema de investigación científica, solo alrededor del 0.1% de todo el oro contenido en la corteza terrestre está disponible, al menos teóricamente, para la minería, pero estas partículas naturales son raras, en su forma natural es monoisotópico y en condiciones normales es inerte a lo orgánico, tiene una red cúbica centrada  y no sufre transformaciones alotrópicas= , se caracteriza por un bajo valor de resistencia a la tracción s - del orden de= 13 - 13.3 kp / mm - y un alto valor de alargamiento - del orden del 50% - en estado recocido. El límite elástico también es muy bajo, es de 0,35 kp / mm= (Boshin et al., 2002)

El método más antiguo para extraer metales raros, basado en la alta densidad d= el oro, es lavar las arenas que las contiene. "La minería ... el lavado de oro requiere solo medios mecánicos, y por lo tanto no es de extrañar que el= oro fuera conocido incluso por los salvajes en los tiempos históricos más antiguos" (D.I. Mendeleev.). Pero la existencia de la hidrometalurgia permite extraer el oro en forma de disoluciones, siendo la lixiviación uno = de los métodos más utilizados, el cianuro es un ejemplo claro de ello, aunque = en los últimos años se han tratado de encontrar otras alternativas.=

 =

Interacción de los metales con ácidos

Casi todos los metales son oxidados por ácidos. En= la mayoría de los casos, las películas protectoras de óxido que exhiben una na= turaleza básica o anfótera son fácilmente solubles en ácidos. Además, el proceso red= ox de la interacción de un metal con un ácido está determinado tanto por la actividad del metal como por la naturaleza y concentración del ácido= (Tretyakov et al. 1993)<= /span>. Los ácidos clorhídrico y sulfúrico diluidos, oxi= dan solo aquellos metales que están en una serie de tensiones al hidrógeno, ya = que el papel del agente oxidante en estos ácidos es desempeñado por los iones de hidrógeno H +, que se reducen a hidrógeno libre (Pustovalova L.M= . y Nikanoroba I.E. 2005)

 

Los átomos de metal tienen pocos electrones en la = capa externa, en la cantidad de 1, 2 o 3. Los metales exhiben propiedades electropositivas y tienen baja electronegatividad, menos de dos. Para la in= teracción de los ácidos con el metal, se deben cumplir ciertas condiciones (en contra= ste con las reacciones de los ácidos con bases y óxidos básicos, que ocurren ca= si siempre). Primero, el metal debe ser suficientemente activo (reactivo) con respecto a los ácidos. Por ejemplo, el oro, la plata, el cobre, el mercurio= y algunos otros metales, con la liberación de hidrógeno no reaccionan con los ácidos. Los metales como el sodio, el calcio y el zinc, por el contrario, reaccionan muy activamente con la liberación de hidrógeno gaseoso y una gran cantidad de calor. Según la reactividad con respecto a los ácidos, todos los metales están dispuestos en una serie de actividad metálica. A la izquierda están los metales más activos, a la derecha están inactivos. Cuanto más a la izquierda hay un metal en una serie de actividades, más intensamente intera= ctúa con los ácidos. En segundo lugar, el ácido debe ser lo suficientemente fuer= te como para reaccionar con el metal. Por la fuerza de un ácido se entiende su capacidad para dar iones de hidrógeno H +. Por ejemplo, los ácid= os vegetales (málico, cítrico, oxálico, etc.) son ácidos débiles y reaccionan = muy lentamente con metales como zinc, cromo, hierro, níquel, estaño, plomo (aun= que pueden reaccionar con bases y óxidos metálicos) (Karapetyants M.Kh. y Draki= n S.I. 2000).

 

Agua regia

Es un agente oxidante particularmente fuerte formado por la mezcla de ácido nítrico y ácido clorhídrico con concentraciones del 65% y 35% respectivamen= te, en una proporción de una a tres partes por volumen (Kreshkov A.P. y Yaroslavtsev A.A. 1960). La unión de HCl y HNO3 produce una mezc= la compleja de productos altamente activos, incluidos los asociados, dióxido de nitrógeno, cloro y cloruro de nitrosilo, esta se prepara inmediatamente ant= es de su uso: durante el almacenamiento, se descompone fácilmente y es poco estable formando productos gaseosos, la formación de dióxido de nitrógeno y cloruro de nitrosilo da el color del agua regia siendo este un líquido amar= illo con olor a cloro y óxidos de nitrógeno.

La efectividad del agua regia como agente oxidante se asocia en gran medida con una disminución en el potencial de oxidación del metal debido a la formació= n de compuestos complejos de cloro. La formación de este complejo oxidante en un entorno fuertemente ácido permite disolver incluso metales de baja actividad como el oro, el platino y el paladio, incluso a temperatura ambiente (Mihaylenko Y. I. 1970)

El mecanismo de formación del agua regia se puede representar de la siguiente manera.

 

·      =    El ácido nítrico HNO3 oxida al ácido clorhídrico HCl, siendo un pro= ceso reversible el cual procede de acuerdo con la ecuación (1).

 

HNO3 + 3HCl ßà NOCl + Cl2 + 2H2O (1)

 

·      =    Se habla del agua regia como un agente oxidante muy fuerte debido al cloruro de nitrosilo (NOCl), que se descompone con la liberación de cloro atómico:

 

2NOCl ßà 2NO + Cl2 (2)

 

Debido a esta liberación se disuelve la mayoría de los metales, incluido el oro, p= or lo que los alquimistas lo llamaron agua regia, ya que el oro era considerad= o el "rey de los metales".

 

No disuelve rodio (Rh), tántalo (Ta), iridio (Ir) y titanio (Ti). <= /span>

 

Durante la interacción del oro con el agua regia, el cloruro de nitrosilo se descom= pone en óxido nítrico y cloro atómico, el cual oxida los átomos y iones de oro. =

 

Au + NOCl ßàAuCl + NO (3)

 

Después ocurre una nueva reacción redox, formando cloruro de oro:=

 

AuCl + Cl2=  ßà AuCl3 (4)

 

El cloruro de oro resultante se une inmediatamente con otra molécula de HCl, formando tetracloroácido, que se lo conoce comúnmente como "oro de cloro":

 

Au= Cl3 + HCl ßàH(AuCl4) (5)

 

Este complejo ácido se cristaliza con cuatro moléculas de agua en forma de H(AuC= l4). 4H2O. Sus cristales son de color amarillo claro; la solución acu= osa también es de color amarillo. Si se calienta cuidadosamente con ácido clorhídrico, se descompone con la liberación de HCl y cristales de color ma= rrón rojizo de cloruro de oro (III) AuCl3. Todos los compuestos de or= o se descomponen fácilmente cuando se calientan para liberar oro metálico (Dimova M.C. y Malinina R. D. 1989).

 

La ecuación de reacción total del oro con el agua regia es:<= /p>

 

Au + 4HCl + HNO3= ßà H[AuCl4] + NO + 2Н2О <= /span>(6)

 

Incluso Geber, un alquimista árabe de la Edad Media, demostró que el cloro es el pr= incipal elemento en el agua regia. El que queda en el aire o durante el almacenamie= nto a largo plazo se evapora y deja de actuar sobre el oro. La velocidad de disolución del oro en agua regia es de aproximadamente 10 μm / min (Metelskaya G.C. et al. 1980).

 

Metodología.

En el presente trabajo de investigación se evaluó la efectividad de 2 reactivos precipitantes utilizados de forma clásica en la recuperación del oro frente= a dos especies poco comunes (azúcar y almidón).

Para cada reactivo se generaron 5 repeticiones determinando un promedio general de cementación, en los ensayos se utilizó 30 gramos de material arenoso de río, añadiendo un g= ramo de una muestra previamente pesada de oro de aluvión con una granulometría e= n el orden de 20 a 200 micras. El análisis de los resultados se logra en el prog= rama Rstudio.

Preparación de la muestra.

La limpieza de la mue= stra se llevó a cabo mediante ebullición en ácido nítrico, filtrando posteriorme= nte el material, después de la limpieza, se agrega ácido clorhídrico HCl en una proporción de volumen 3:1 con diferencia al ácido nítrico. En este caso, el= oro se disuelve solo en ácido clorhídrico. Ni el nitrógeno ni el oxígeno están incluidos en el ácido clorhídrico, luego se calienta la mezcla y agrega gradualmente el ácido nítrico y una vez finalizada la disolución, debe mantenerse la disolución calentada durante aproximadamente media hora. El á= cido nítrico actúa solo como un agente oxidante, catalizando la entrada de oro e= n la reacción.

Lo principal es no exagerar con ácido nítrico, ya que, al precipitar el oro de una solución, s= erá necesario deshacerse de él de manera más consistente.

La lixiviación del or= o

Esta se logra con el = agua regia, se filtra la solución a través de papel de filtro dejando reposar durante 20-30 minutos. La mayoría de los componentes volátiles se evaporará= n y la evaporación llevará menos tiempo, luego, se debe agregar ácido sulfúrico= en un volumen del 5% al de la muestra y se procede con la evaporación de agua regia.

La solución debe evaporarse cuidadosamente, calentando lentamente, pero sin hervir. Cuando se vuelve almibarado, se agrega más ácido clorhídrico y se continúa evaporando, luego, nuevamente agregamos HCl a la consistencia inicial, y la mezcla resultante se diluye con agua en una proporción de 1:1. Dejamos la solución durante 24 horas en un lugar fresco. Los residuos se depositarán en el fond= o. Se filtra cuidadosamente la solución para eliminar los sedimentos y la turbidez.

Precipitación por med= io del bisulfito de sodio

La solución que conte= nía oro se alcalinizó con urea hasta un ph mayor a 10, luego se agregó 0.79 gra= mos de bisulfito de sodio por cada gramo de oro disuelto y se calentó en baño m= aría por una hora, los residuos son lavados con agua destilada, para ser filtrado con papel filtro para ser calcinados.

Precipitación por med= io de sulfato ferroso

Sobre la solución de = AuCl3 obtenida de la forma ya descrita anteriormente y contenida en un vaso precipitado, se le agrega la disolución de caparrosa preparada con 5gr de sulfato ferroso disuelto en 40ml de agua destilada y acidificada al 10% de = ácido sulfúrico, se deja reposar por 30 min y se filtra, el filtro se lava con ác= ido clorhídrico, agua destilada, agua amoniacal y nuevamente con agua destilada= , se seca el filtro en una estufa a 70 °C, se calcina y se pesa la muestra.

Precipitación por medio del Azúcar

 

Utilizando la solución donde se encuentra disuelto el oro, es necesario alcalinizar a = un pH de 11-12, esto se logra con carbonato de calcio carbonizado, para esto se calcina el bicarbonato de sodio y se prepara una alta concentración con agua destilada, se filtra y se agrega 7 gramos de sacarosa por cada gramo de oro= se lleva a ebullir y después de un tiempo el oro precipita y se calcina.<= /o:p>

 

Precipitación por medio del Almidón

Para realizar la precipitación con almidón se prepara una solución al 1% = en una solución de NaCl al 0.= 3%, y por cada 5ml de dicha solución se agrega 1 ml de saliva, para que la enzima amilasa salival pueda transformarla en dextrina a una temperatura de 38°C, = por un tiempo alrededor de 20 min o hasta que la prueba del yodo salga negativa= .

Para precipitar el oro se agrega 1 ml a nuestra solución del agua regia y se lle= va a ebullición se deja reposar por 48 horas se filtra y se calcina.<= /span>

 

Resultados.

El oro obtenido luego de su precipitación para todas las repeticiones con cada reactivo empleado, se le aplicó el proceso de calcinado obteniendo así el p= eso total de oro para cada muestra, los cuales se representan en la tabla 1.

Al determinar el prom= edio general de oro precipitado por los reactivos permitió observar el rendimien= to y efectividad de estos, siendo el azúcar el reactivo más efectivo al precipit= ar la mayor cantidad de oro.

Tabla 1 – Resultado de oro precipitado de los ensayos con los diferentes reactivos

 

Muestra

Oro agregado (gr)

Oro precipitado con Bisulfito de Sodio (gr)

Oro precipitado con Sulfato Ferroso (gr)=

Oro precipitado con Azúcar (gr)

Oro precipitado con Almidón (gr)

1

1

0.958

0.958

0.956

0.702

2

1

0.943

0.964

0.984

0.683

3

1

0.932

0.976

0.967

0.703

4

1

0.956

0.956

0.964

0.674

5

1

0.963

0.974

0.985

0.686

&nbs= p;

Promedio<= o:p>

= 0.9504

= 0.9656

= 0.9712

= 0.6896

 

Fuente: Elaborado por los autores

Los datos que arroja = la tabla 1 fueron introducidos en un software de programación estadístico llam= ado Rstudio, realizando en este un análisis de varianza.

Para analizar las relaciones entre las repeticiones realizadas para cada reactivo se realizó = un diagrama de dispersión el cual se muestra en el gráfico 1, este nos indica = que cada reactivo posee una correlación moderada entre sus repeticiones, así co= mo que los reactivos bisulfito de sodio, sulfato ferroso y azúcar presentan rendimiento elevado con promedios semejantes en precipitación frente al alm= idón.

Figura 1. Oro recuperado con diferentes reactivos

Fuente: Elaborado por los autores

 

En el programa Rstudio se ingresaron los comandos respectivos para la realización del análisis de la varianza ANOVA con la variable independiente “Oro recuperado” frente a la variable categórica “Reactivo” dando los siguientes resultados:

Terms:

              =    Reactivo Residuals

Sum of Squares  0.2802328 0.0022604

Deg. of Freedom         3        16

 

Residual standard error: 0.01188592<= /span>

 

El programa muestra la suma de los cuadrados y los grados de libertad para los datos ingresados, para determinar el nivel de significancia se ingresó un nuevo comando dando los siguientes resultados:<= /span>            Df  Sum Sq Mean Sq F value Pr(>F)   

Reactivo     3 0.28023 0.09341   661.2 <2e-16 ***

Residuals   16 0.00226 0.00014                  

---

= Signif. codes:  0 ‘***’ 0.001 ‘**’ 0.01 ‘*’= 0.05 ‘.’  

Los datos indican que la prueba si es significativ= a y que las medias de las repeticiones para cada reactivo son diferentes, para determinar estadísticamente la diferencia de la cantidad de oro recuperado = se aplica la prueba de Tukey.

  Tukey multiple comparisons of means<= /o:p>

    95% family-wise confidence level

 

Fit: aov(formula =3D `Oro recuperado (gr)` ~ Reactivo)

 

$Reactivo

                                diff          lwr          upr     p adj

= Azucar-Almidon                0.2816  0.260092817 0.3031071825 0.0000000=

Bisulfito de Sodio-Almidon    0.2608  0.239292817 0.2823071825 0.0000000

Sulfato Ferroso-Almidon       0.2760  0.254492817 0.2975071825 0.0000000

Bisulfito de Sodio-Azucar    -0.0208 -0.042307183 0.0007071825 0.0= 598138

Sulfato Ferroso-Azucar       -0.0056 -0.027107183 0.0159071825 0.8774619

Sulf. Ferr.-Bisulf. de Sodio  0.0152 -0.006307183 0.0367071825 0.2210= 647

Los resultados muestran las diferencias de las med= ias para cada reactivo con su intervalo respectivo y los valores para cada contraste, al comparar las medias del almidón frente a las medias de los de= más reactivos se observa que existe una gran diferencia en el porcentaje de oro recuperado, mientras que los demás reactivos presentan similares porcentaje= s de recuperación, en la figura 2 se muestra un diagrama de cajas donde se obser= va un resumen de lo descrito.

Figura 2. Comparación de oro recuperado con diferentes reactivos.

Fuente: Elaborado por los autores

Conclusiones.

·      =    La hidromet= alúrgica es un proceso de extracción de metales mediante reacciones químicas en soluciones acuosas. Como materias primas, se pueden usar minerales, concentrados químicos, desechos de otras industrias o procesos hidrometalúrgicos. Este método es útil cuando la materia prima contenga una baja concentración de metal y no pueda procesarse por métodos tradicionales. Las características positivas de la hidrometalurgia incluyen la posibilidad= de separación de metales de propiedades similares y una opción de procesamiento más simplificada.

·      =    En la actua= lidad existen diferentes reactivos usados de forma clásica en la recuperación de = oro de soluciones, pero nuevos trabajos de investigación presentan una amplia variedad de nuevos agentes precipitantes mas accesibles como es el caso del azúcar y el almidón.

·      =    En las prue= bas realizadas se observa que el azúcar presenta un gran rendimiento en la precipitación del oro, pero para esto la solución debe de tener un pH de 11= -12.

·      =    El almidón = puede llevar a ser agente precipitante del oro disuelto si se sintetiza adecuadam= ente en forma de dextrina con enzimas específicas.

 

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PARA CITAR EL ARTÍCULO INDEXADO.

 

 

Briones García, J. I., Toledo Castillo, N. del R., & Mejía Reinoso, T. J. (2020). Evaluación de diferentes reactivos aplicados en la precipitación del oro . ConcienciaD= igital, 3(2.1), 199-209. https://doi= .org/10.33262/concienciadigital.v3i2.1.1234

 

 



 

 

 

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El artículo queda en propiedad de= la revista y, por tanto, su publicación parcial y/o total en otro medio tiene = que ser autorizado por el director de la Revista Conciencia Digital.

 

 

 

 



[1]Escuela Superior Politécnica de Chimborazo, Sede Morona Santiago. Macas, Ecuador. j= avier.briones@espoch.edu.ec

[2] Escuela Superior Politécnica de Chimborazo, Sede Morona Santiago. Ma= cas, Ecuador. toledo@espoch.edu.ec

[3] Escuela Superior Politécnica de Chimborazo, Maestría en química aplicada, Estudiante de posgrado. Macas, Ecuador. jmejiareinoso@yahoo.com

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                                                 =                                                                       ISSN: 2600-5859

                               =                                                        Vol. 3, N°2.1, p. 199-209, mayo, 2020

 

Creatividad & Desarrol= lo                                                =                                                 =                              Página 199=

 

 

 

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